3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl alcohol

Base Information

• Chemical Name: 3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl alcohol
• CAS No.: 288850-05-5
• Molecular Formula: C₁₀₅H₁₅₆O₃₉
• Molecular Weight: 2042.37
• Mol file: 288850-05-5.mol

Synonyms:3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl alcohol

Chemical Property of 3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl alcohol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl alcohol

There total 1 articles about 3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

5-(hydroxymethyl)benzene-1,3-diol (29654-55-5) + 3,5-di-(3',5'-di-[1'',4'',7'',10''-tetraoxaundecyl]benzyloxy)benzyl bromide (288850-04-4) → 3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl alcohol (288850-05-5)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; In acetone; for 18h; Heating;

DOI:10.1039/b002026p

Reference yield: 85.0%

3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl alcohol (288850-05-5) → 3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl bromide (288850-06-6)

Guidance literature:

With phosphorus tribromide; In benzene; at 20 ℃; for 6h; Cooling with ice;

DOI:10.1002/chem.201300289

Reference yield: 82.0%

3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl alcohol (288850-05-5) → (C21H35O9)4(C7H5O)2C6H3CHO

Guidance literature:

With manganese(IV) oxide; In dichloromethane;

DOI:10.1039/b203272b

upstream raw materials:

5-(hydroxymethyl)benzene-1,3-diol

3,5-di-(3',5'-di-[1'',4'',7'',10''-tetraoxaundecyl]benzyloxy)benzyl bromide

Downstream raw materials:

3,5-di-(3',5'-di-(3'',5''-di-[1''',4''',7''',10'''-tetraoxaundecyl]benzyloxy)-benzyloxy)benzyl bromide