Technology Process of C52H75O12P
There total 6 articles about C52H75O12P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; dmap;
In
dichloromethane;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1016/j.bmc.2013.04.027
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: pyridine; dmap / -78 - 20 °C / Inert atmosphere
2.1: tin(IV) chloride / dichloromethane / -78 °C / Inert atmosphere
3.1: dimethylsulfide borane complex / tetrahydrofuran / 0 °C / Inert atmosphere
3.2: 0 - 20 °C
4.1: pyridine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere
With
pyridine; dmap; dimethylsulfide borane complex; tin(IV) chloride;
In
tetrahydrofuran; dichloromethane;
2.1: |Sakurai Allylation;
DOI:10.1016/j.bmc.2013.04.027
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere
2.1: pyridine; dmap / -78 - 20 °C / Inert atmosphere
3.1: tin(IV) chloride / dichloromethane / -78 °C / Inert atmosphere
4.1: dimethylsulfide borane complex / tetrahydrofuran / 0 °C / Inert atmosphere
4.2: 0 - 20 °C
5.1: pyridine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere
With
pyridine; dmap; dimethylsulfide borane complex; tin(IV) chloride; diisobutylaluminium hydride;
In
tetrahydrofuran; dichloromethane;
3.1: |Sakurai Allylation;
DOI:10.1016/j.bmc.2013.04.027