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C22H30O4

Base Information Edit
C<sub>22</sub>H<sub>30</sub>O<sub>4</sub>

Synonyms:C22H30O4

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of C22H30O4 Edit
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Technology Process of C22H30O4

There total 3 articles about C22H30O4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 2.5h;
DOI:10.1016/j.bmcl.2011.12.137
Guidance literature:
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: pyridinium chlorochromate / dichloromethane / 2.5 h / 20 °C
With sodium hydride; pyridinium chlorochromate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.12.137
Guidance literature:
Multi-step reaction with 3 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 4 h / Inert atmosphere; Reflux
2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
3.1: pyridinium chlorochromate / dichloromethane / 2.5 h / 20 °C
With lithium aluminium tetrahydride; sodium hydride; pyridinium chlorochromate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.12.137
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