C₂₂H₃₀O₄

Base Information

• Chemical Name: C₂₂H₃₀O₄
• CAS No.: 1360998-97-5
• Molecular Formula: C₂₂H₃₀O₄
• Molecular Weight: 358.478
• Mol file: 1360998-97-5.mol

Synonyms:C₂₂H₃₀O₄

Chemical Property of C₂₂H₃₀O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₃₀O₄

There total 3 articles about C₂₂H₃₀O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H32O4 (1360998-95-3) → C22H30O4 (1360998-97-5)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 2.5h;

DOI:10.1016/j.bmcl.2011.12.137

Reference yield:

Bicyclo<2.2.2>octane-1,4-dimethanol (826-45-9) → C22H30O4 (1360998-97-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: pyridinium chlorochromate / dichloromethane / 2.5 h / 20 °C

With sodium hydride; pyridinium chlorochromate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.12.137

Reference yield:

Bicyclo<2.2.2.>octan-1,4-dicarbonsauere-ethylester (1659-75-2) → C22H30O4 (1360998-97-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 4 h / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: pyridinium chlorochromate / dichloromethane / 2.5 h / 20 °C

With lithium aluminium tetrahydride; sodium hydride; pyridinium chlorochromate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.12.137

upstream raw materials:

C₂₂H₃₂O₄

Bicyclo<2.2.2>octane-1,4-dimethanol

Bicyclo<2.2.2.>octan-1,4-dicarbonsauere-ethylester

Downstream raw materials:

C₂₈H₄₂O₅

C₃₀H₄₈O₄

C₂₈H₃₈O₅

Refernces