8-methoxycarbonyloct-1-yl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:8-methoxycarbonyloct-1-yl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside
CAS No.:56343-03-4
Molecular Formula:C₂₅H₃₇NO₈
Molecular Weight:479.571
Hs Code.:

Synonyms:8-methoxycarbonyloct-1-yl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

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Chemical Property of 8-methoxycarbonyloct-1-yl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Chemical Property:

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Technology Process of 8-methoxycarbonyloct-1-yl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

There total 11 articles about 8-methoxycarbonyloct-1-yl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 82812-32-6
9-((2S,3R,4R,5S,6R)-3-Acetylamino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-nonanoic acid methyl ester

: 56343-03-4,71048-95-8,79083-28-6,82863-54-5
9-((2R,4aR,6S,7R,8R,8aS)-7-Acetylamino-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-6-yloxy)-nonanoic acid methyl ester

Guidance literature:: With toluene-4-sulfonic acid; at 25 ℃;
DOI:10.1016/S0008-6215(82)80027-X

Reference yield:

: dimethoxytoluene (benzaldehyde dimethyl acetal)

: 3068-34-6,41355-44-6,51236-40-9,74081-14-4,79897-03-3,100759-09-9,109581-83-1,38874-23-6
2-Acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl chloride

: 34957-73-8
methyl 9-hydroxynonanoate

: 65567-18-2
8-methoxycarbonyloctyl 2-acetamido-2-deoxy-β-D-glucopyranoside

: 8-methoxycarbonyloctyl-2-acetamido-4,6-di-benzylidene-2-deoxy-β-D-glucopyranoside

: 56343-03-4
8-methoxycarbonyloct-1-yl 2-acetamido-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside

Guidance literature:: With potassium iodide; sodium; sodium hydrogencarbonate; toluene-4-sulfonic acid; mercury(II) cyanide; In N-methyl-acetamide; methanol; dichloromethane;

Reference yield:

: 67817-37-2
3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl chloride

: 56343-03-4,71048-95-8,79083-28-6,82863-54-5
8-methoxycarbonyloctyl 2-acetamido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: mercuric cyanide / benzene; nitromethane / 72 h / 45 - 50 °C

2: H₂ / Pd/C(5percent) / acetic acid / 4 h

3: 2) sodium methoxide / 1) toluene; 2) methanol

4: p-toluenesulfonic acid / dimethylformamide / 5 h / 50 °C

With hydrogen; sodium methylate; mercury(II) cyanide; toluene-4-sulfonic acid; palladium on activated charcoal; In nitromethane; acetic acid; N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0008-6215(00)80750-8