2-(1-([1,1'-biphenyl]-4-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(1-([1,1'-biphenyl]-4-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1070704-01-6
Molecular Formula:C₂₀H₂₅BO₂
Molecular Weight:308.228
Hs Code.:

Synonyms:2-(1-([1,1'-biphenyl]-4-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(1-([1,1'-biphenyl]-4-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(1-([1,1'-biphenyl]-4-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 5 articles about 2-(1-([1,1'-biphenyl]-4-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 2350-89-2
p-vinylbiphenyl

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1070704-01-6
2-(1-([1,1'-biphenyl]-4-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With C₃₄H₃₀NiO₆; potassium; In tetrahydrofuran; at 25 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c9dt00468h

Reference yield: 85.0%

: 2350-89-2
p-vinylbiphenyl

: 73183-34-3
bis(pinacol)diborane

: 1070704-01-6
2-(1-([1,1'-biphenyl]-4-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With methanol; C₁₉H₂₁ClNNiOP; potassium acetate; In toluene; at 25 ℃; for 24h; regioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.0c01416

Reference yield: 78.0%

: 2350-89-2
p-vinylbiphenyl

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1070704-01-6
2-(1-([1,1'-biphenyl]-4-yl)ethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 4,4,5,5-tetramethyl-(2,2([1,1’-biphenyl]4-yl)ethyl)-1,3,2-dioxaborolane

Guidance literature:: With dmap; chloro(1,5-cyclooctadiene)rhodium(I) dimer; 1,4-di(diphenylphosphino)-butane; In 1,2-dichloro-ethane; at 20 ℃; for 0.166667h; regioselective reaction;
DOI:10.1055/s-0028-1087415