5-(benzyloxycarbonyl)amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one

Base Information

• Chemical Name: 5-(benzyloxycarbonyl)amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one
• CAS No.: 223718-58-9
• Molecular Formula: C₂₆H₁₉N₃O₄
• Molecular Weight: 437.455

Synonyms:5-(benzyloxycarbonyl)amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one

Chemical Property of 5-(benzyloxycarbonyl)amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one

Chemical Property:

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Technology Process of 5-(benzyloxycarbonyl)amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one

There total 2 articles about 5-(benzyloxycarbonyl)amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1,3-diphenyl-5-oxo-4,5-dihydro-1H-pyrazole (4845-49-2) + Methyl (Z)-2-<(benzyloxycarbonyl)amino>-3-dimethylaminopropenoate (219739-90-9) → 5-(benzyloxycarbonyl)amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one (223718-58-9)

Guidance literature:

In acetic acid; for 4.5h; Heating;

DOI:10.1002/jhet.5570360135

Reference yield:

N-(Benzyloxycarbonyl)glycine (1138-80-3) → 5-(benzyloxycarbonyl)amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one (223718-58-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 94 percent / thionyl chloride / 2 h / 0 °C

2: 96 percent / toluene / 1 h / 100 °C

3: 93 percent / acetic acid / 4.5 h / Heating

With thionyl chloride; In acetic acid; toluene;

DOI:10.1002/jhet.5570360135

Reference yield: 91.0%

5-(benzyloxycarbonyl)amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one (223718-58-9) → 5-amino-1,3-diphenyl-1H,6H-pyrano<2,3-c>pyrazol-6-one

Guidance literature:

With cyclohexene; palladium on activated charcoal; In ethanol; for 1.5h; Heating;

DOI:10.1002/jhet.5570360135

upstream raw materials:

1,3-diphenyl-5-oxo-4,5-dihydro-1H-pyrazole

Methyl (Z)-2-<(benzyloxycarbonyl)amino>-3-dimethylaminopropenoate

N-(Benzyloxycarbonyl)glycine

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