C₁₂H₁₃F₃OS

Base Information

Chemical Name:C₁₂H₁₃F₃OS
CAS No.:1415577-91-1
Molecular Formula:C₁₂H₁₃F₃OS
Molecular Weight:262.296
Hs Code.:

C<sub>12</sub>H<sub>13</sub>F<sub>3</sub>OS

Synonyms:C₁₂H₁₃F₃OS

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Chemical Property of C₁₂H₁₃F₃OS

Chemical Property:

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Technology Process of C₁₂H₁₃F₃OS

There total 3 articles about C₁₂H₁₃F₃OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415577-90-0
C₁₂H₁₅F₃OS

: 1415577-91-1
C₁₂H₁₃F₃OS

Guidance literature:: C₁₂H₁₅F₃OS; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.666667h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 0 ℃; for 7h;

Reference yield:

: 21651-04-7
3-hydroxy-2,2-dimethylpropyl 4-methylbenzenesulfonate

: 1415577-91-1
C₁₂H₁₃F₃OS

Guidance literature:: Multi-step reaction with 2 steps

1.1: 60percent sodium hydrate / N,N-dimethyl-formamide / 0.42 h / Inert atmosphere; Cooling with ice

1.2: 9 h / 10 - 90 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.67 h / -78 °C / Inert atmosphere

2.2: 7 h / -78 - 0 °C

With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 1415577-91-1
C₁₂H₁₃F₃OS

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 3 h / 0 °C

2.1: 60percent sodium hydrate / N,N-dimethyl-formamide / 0.42 h / Inert atmosphere; Cooling with ice

2.2: 9 h / 10 - 90 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.67 h / -78 °C / Inert atmosphere

3.2: 7 h / -78 - 0 °C

With pyridine; oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; N,N-dimethyl-formamide;