tert-butyl (S)-3-phenyl-1-(3-((S)-1-phenylethyl)thioureido)propan-2-ylcarbamate

Base Information

• Chemical Name: tert-butyl (S)-3-phenyl-1-(3-((S)-1-phenylethyl)thioureido)propan-2-ylcarbamate
• CAS No.: 1172597-05-5
• Molecular Formula: C₂₃H₃₁N₃O₂S
• Molecular Weight: 413.584

Synonyms:tert-butyl (S)-3-phenyl-1-(3-((S)-1-phenylethyl)thioureido)propan-2-ylcarbamate

Chemical Property of tert-butyl (S)-3-phenyl-1-(3-((S)-1-phenylethyl)thioureido)propan-2-ylcarbamate

Chemical Property:

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Technology Process of tert-butyl (S)-3-phenyl-1-(3-((S)-1-phenylethyl)thioureido)propan-2-ylcarbamate

There total 2 articles about tert-butyl (S)-3-phenyl-1-(3-((S)-1-phenylethyl)thioureido)propan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

((S)-1-Phenyl-ethyl)-thiourea (25144-91-6) + tert-butyl [(2S)-1-azido-3-phenylpropan-2-yl]carbamate (134557-74-7) → tert-butyl (S)-3-phenyl-1-(3-((S)-1-phenylethyl)thioureido)propan-2-ylcarbamate (1172597-05-5)

Guidance literature:

((S)-1-Phenyl-ethyl)-thiourea; With pyridine; carbon disulfide; In tetrahydrofuran; at 0 ℃; for 0.166667h;

tert-butyl [(2S)-1-azido-3-phenylpropan-2-yl]carbamate; In tetrahydrofuran; at 0 - 20 ℃; for 6h; Inert atmosphere;

DOI:10.1039/c8ob00239h

Reference yield: 70.0%

tert-butyl (S)-1-isothiocyanato-3-phenylpropan-2-ylcarbamate (1172596-81-4) + (S)-1-phenyl-ethylamine (2627-86-3) → tert-butyl (S)-3-phenyl-1-(3-((S)-1-phenylethyl)thioureido)propan-2-ylcarbamate (1172597-05-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃;

DOI:10.1021/jo900675s

upstream raw materials:

tert-butyl (S)-1-isothiocyanato-3-phenylpropan-2-ylcarbamate

(S)-1-phenyl-ethylamine

((S)-1-Phenyl-ethyl)-thiourea

tert-butyl [(2S)-1-azido-3-phenylpropan-2-yl]carbamate

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