ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate)

Base Information

Chemical Name:ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate)
CAS No.:212607-84-6
Molecular Formula:C₂₀H₂₆O₆S₄
Molecular Weight:490.687
Hs Code.:

Synonyms:ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate)

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Technology Process of ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate)

There total 1 articles about ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 5244-34-8
2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol

: 98-59-9
p-toluenesulfonyl chloride

: 212607-84-6
ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate)

Guidance literature:: 2,2'-ethane-1,2-diylbissulfanyl-bis-ethanol; With triethylamine; In dichloromethane; at 20 ℃; for 1h;

p-toluenesulfonyl chloride; In dichloromethane; at 20 ℃;
DOI:10.2174/1570178612666150108001219

Reference yield: 29.0%

: 212607-84-6
ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate)

: 1283056-82-5
bis-1,11-[methyl-2,3-di-O-benzyl-6-deoxy-6-tosyIamino-4-yloxy-α-D-glucopyranoside]-(6-tosyl-3,9-dioxa-6-aza-undecane)

: 1283057-12-4
cyclo-(N,N')-1,8-{bis-1,11-[methyl-2,3-di-O-benzyl-6-deoxy-6-tosylamino-4-yloxy-α-D-glucopyranoside]-(6-tosyl-3,9-dioxa-6-aza-undecane)}-(3,6-dithia-octane)

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 72h;
DOI:10.1016/j.crci.2010.03.032

Reference yield:

: 21645-25-0
phenol 2-[(tetrahydro-2H-pyran-2yl)oxy]

: 212607-84-6
ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate)

: C₂₈H₃₈O₆S₂

Guidance literature:: phenol 2-[(tetrahydro-2H-pyran-2yl)oxy]; With caesium carbonate; In acetonitrile; for 0.5h; Reflux; Inert atmosphere;

ethan-1,2-diylbis(bis(sulfanediyl))bis(ethan-2,1-diyl) bis(4-methylbenzenesulfonate); In acetonitrile; for 36h; Reflux; Inert atmosphere;
DOI:10.2174/1570178612666150108001219