(3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one

Base Information

Chemical Name:(3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one
CAS No.:87014-18-4
Molecular Formula:C₁₆H₂₀O₅
Molecular Weight:292.332
Hs Code.:

Synonyms:(3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one

Suppliers and Price of (3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of (3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one

There total 1 articles about (3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87014-17-3
Acetic acid (1R,3S,6S)-6-(3,4-dimethoxy-phenyl)-8-oxo-bicyclo[4.2.0]oct-3-yl ester

: 87014-18-4
(3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; Yield given;
DOI:10.1021/jo00169a068

Reference yield: 86.0%

: 87014-18-4
(3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one

: 87014-19-5
(3aR,7aR)-3a-(3,4-Dimethoxy-phenyl)-hexahydro-benzofuran-2,6-dione

Guidance literature:: With pyridinium chlorochromate;
DOI:10.1021/jo00169a068

Reference yield:

: 87014-18-4
(3aR,6S,7aR)-3a-(3,4-Dimethoxy-phenyl)-6-hydroxy-hexahydro-benzofuran-2-one

: 21104-34-7
N-methyl-3a-<3,4-(dimethoxy)phenyl>-2,3,3a,4,5,6,7,7a-octahydroindole-2,6-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / pyridinium chlorochromate

2: ethanol

3: oxalyl chloride / benzene

4: methanol / Ambient temperature

With oxalyl dichloride; pyridinium chlorochromate; In methanol; ethanol; benzene;
DOI:10.1021/jo00169a068