Technology Process of C55H66F26O7
There total 6 articles about C55H66F26O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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1358816-97-3
5-hydroxy-isophthalic acid bis-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl) ester
- Guidance literature:
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With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 0 ℃;
Inert atmosphere;
Reflux;
DOI:10.1039/c1nj20530g
- Guidance literature:
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Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C
2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux
With
di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; triphenylphosphine;
In
tetrahydrofuran;
2: Mitsunobu etherification;
DOI:10.1039/c1nj20530g
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 12 h / 57 °C / Inert atmosphere
2: acetic acid / tetrahydrofuran; water / 3 h
3: 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide / tetrahydrofuran; dichloromethane / 0 - 25 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C
5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux
With
1H-imidazole; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; 4-pyrrolidin-1-ylpyridine; acetic acid; dicyclohexyl-carbodiimide; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
5: Mitsunobu etherification;
DOI:10.1039/c1nj20530g
