(4-Methoxymethoxy-phenyl)-(2-oxo-azetidin-1-yl)-acetic acid benzhydryl ester

Base Information

Chemical Name:(4-Methoxymethoxy-phenyl)-(2-oxo-azetidin-1-yl)-acetic acid benzhydryl ester
CAS No.:78771-66-1
Molecular Formula:C₂₆H₂₅NO₅
Molecular Weight:431.488
Hs Code.:

Synonyms:(4-Methoxymethoxy-phenyl)-(2-oxo-azetidin-1-yl)-acetic acid benzhydryl ester

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Chemical Property of (4-Methoxymethoxy-phenyl)-(2-oxo-azetidin-1-yl)-acetic acid benzhydryl ester

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Technology Process of (4-Methoxymethoxy-phenyl)-(2-oxo-azetidin-1-yl)-acetic acid benzhydryl ester

There total 3 articles about (4-Methoxymethoxy-phenyl)-(2-oxo-azetidin-1-yl)-acetic acid benzhydryl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 78829-76-2
N-Benzhydryl-2-(4-methoxymethoxy-phenyl)-2-(2-oxo-azetidin-1-yl)-acetamide

: 78771-66-1
(4-Methoxymethoxy-phenyl)-(2-oxo-azetidin-1-yl)-acetic acid benzhydryl ester

Guidance literature:: With sodium acetate; dinitrogen tetraoxide; In chloroform; at 0 ℃; for 1h;
DOI:10.1055/s-1981-29461

Reference yield:

: 6744-65-6
N-benzhydrylformamide

: 78771-66-1
(4-Methoxymethoxy-phenyl)-(2-oxo-azetidin-1-yl)-acetic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / Thionyl chloride / dimethylformamide / 0.5 h / -55 - -35 °C

2: 47 percent / methanol; H₂O / 25 °C

3: 83 percent / Dinitrogen tetroxide, sodium acetate / CHCl₃ / 1 h / 0 °C

With thionyl chloride; sodium acetate; dinitrogen tetraoxide; In methanol; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1055/s-1981-29461

Reference yield:

: 3128-85-6
diphenylmethyl isocyanide

: 78771-66-1
(4-Methoxymethoxy-phenyl)-(2-oxo-azetidin-1-yl)-acetic acid benzhydryl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 47 percent / methanol; H₂O / 25 °C

2: 83 percent / Dinitrogen tetroxide, sodium acetate / CHCl₃ / 1 h / 0 °C

With sodium acetate; dinitrogen tetraoxide; In methanol; chloroform; water;
DOI:10.1055/s-1981-29461