3,3-dicarbonyl-3-(η(5)-cyclopentadienyl)-2,2-diphenyl-1-thia-2λ(4)-phospha-3-molybdacyclopropane

Base Information

Chemical Name:3,3-dicarbonyl-3-(η(5)-cyclopentadienyl)-2,2-diphenyl-1-thia-2λ(4)-phospha-3-molybdacyclopropane
CAS No.:76380-95-5
Molecular Formula:C₁₉H₁₅MoO₂PS
Molecular Weight:434.307
Hs Code.:

Synonyms:3,3-dicarbonyl-3-(η(5)-cyclopentadienyl)-2,2-diphenyl-1-thia-2λ(4)-phospha-3-molybdacyclopropane

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Chemical Property of 3,3-dicarbonyl-3-(η(5)-cyclopentadienyl)-2,2-diphenyl-1-thia-2λ(4)-phospha-3-molybdacyclopropane

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Technology Process of 3,3-dicarbonyl-3-(η(5)-cyclopentadienyl)-2,2-diphenyl-1-thia-2λ(4)-phospha-3-molybdacyclopropane

There total 5 articles about 3,3-dicarbonyl-3-(η(5)-cyclopentadienyl)-2,2-diphenyl-1-thia-2λ(4)-phospha-3-molybdacyclopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 12128-23-3
tricarbonylcyclopentadienylmolybdenum(II) chloride

: 6591-07-7
diphenylphosphane sulfide

: 76380-95-5
3,3-dicarbonyl-3-(η(5)-cyclopentadienyl)-2,2-diphenyl-1-thia-2λ(4)-phospha-3-molybdacyclopropane

Guidance literature:: With (C₂H₅)3N; In benzene; byproducts: (C2H5)3NHCl; refluxing for 4h with an excess of (C2H5)3N under N2; filtration ((C2H5)3NHCl); separation with n-hexane; elem. anal.;

Reference yield: 74.7%

: 172538-02-2
4,4-dicarbonyl-4-(η(5)-cyclopentadienyl)-5,5-diphenyl-2-(2,4,6-trimethylphenyl)-1,3-dithia-2λ(5),5λ(4)-diphospha-3-molybdacyclopentane-2-thione

: 76380-95-5
3,3-dicarbonyl-3-(η(5)-cyclopentadienyl)-2,2-diphenyl-1-thia-2λ(4)-phospha-3-molybdacyclopropane

Guidance literature:: In tetrahydrofuran; (argon); reflux (10 h); solvent removal (vac.), column chromy. (basic alumina; Et2O), collection, concn. (vac.), pptn. with n-hexane, filtration, washing (n-hexane), drying (vac.); elem. anal.;