2-amino-4-(2'-chloro-5'-nitrophenyl)-4,10-dihydro[1,3,5]triazino[1,2-a]benzimidazole hydrochloride

Base Information

Chemical Name:2-amino-4-(2'-chloro-5'-nitrophenyl)-4,10-dihydro[1,3,5]triazino[1,2-a]benzimidazole hydrochloride
CAS No.:1354574-50-7
Molecular Formula:C₁₅H₁₁ClN₆O₂*ClH
Molecular Weight:379.205
Hs Code.:

Synonyms:2-amino-4-(2'-chloro-5'-nitrophenyl)-4,10-dihydro[1,3,5]triazino[1,2-a]benzimidazole hydrochloride

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Chemical Property of 2-amino-4-(2'-chloro-5'-nitrophenyl)-4,10-dihydro[1,3,5]triazino[1,2-a]benzimidazole hydrochloride

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Technology Process of 2-amino-4-(2'-chloro-5'-nitrophenyl)-4,10-dihydro[1,3,5]triazino[1,2-a]benzimidazole hydrochloride

There total 3 articles about 2-amino-4-(2'-chloro-5'-nitrophenyl)-4,10-dihydro[1,3,5]triazino[1,2-a]benzimidazole hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 774560-40-6
C₁₅H₁₁ClN₆O₂

: 1354574-50-7
2-amino-4-(2'-chloro-5'-nitrophenyl)-4,10-dihydro[1,3,5]triazino[1,2-a]benzimidazole hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; for 24h; Cooling with ice;
DOI:10.1016/j.molstruc.2011.10.054

Reference yield:

: 5418-95-1
2-guanidinobenzimidazole

: 1354574-50-7
2-amino-4-(2'-chloro-5'-nitrophenyl)-4,10-dihydro[1,3,5]triazino[1,2-a]benzimidazole hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 3 h / Reflux

2: hydrogenchloride / ethanol / 24 h / Cooling with ice

With piperidine; hydrogenchloride; In ethanol;
DOI:10.1016/j.molstruc.2011.10.054

Reference yield:

: 16634-91-6
2-methyl-5-nitro-benzaldehyde

: 1354574-50-7
2-amino-4-(2'-chloro-5'-nitrophenyl)-4,10-dihydro[1,3,5]triazino[1,2-a]benzimidazole hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 3 h / Reflux

2: hydrogenchloride / ethanol / 24 h / Cooling with ice

With piperidine; hydrogenchloride; In ethanol;
DOI:10.1016/j.molstruc.2011.10.054