tetraethyl N-[(3,4-dihydroxyphenylpropyl)amino]methylbisphosphonate

Base Information

Chemical Name:tetraethyl N-[(3,4-dihydroxyphenylpropyl)amino]methylbisphosphonate
CAS No.:740083-66-3
Molecular Formula:C₁₈H₃₃NO₈P₂
Molecular Weight:453.409
Hs Code.:

Synonyms:tetraethyl N-[(3,4-dihydroxyphenylpropyl)amino]methylbisphosphonate

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Chemical Property of tetraethyl N-[(3,4-dihydroxyphenylpropyl)amino]methylbisphosphonate

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Technology Process of tetraethyl N-[(3,4-dihydroxyphenylpropyl)amino]methylbisphosphonate

There total 3 articles about tetraethyl N-[(3,4-dihydroxyphenylpropyl)amino]methylbisphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.8%

: tetraethyl (E)-N-[3-(3,4-dibenzyloxyphenylprop-2-enylidene)amino]methylbisphosphonate

: 2525-02-2
4-propylbenzene-1,2-diol

: 740083-66-3
tetraethyl N-[(3,4-dihydroxyphenylpropyl)amino]methylbisphosphonate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 4h; atmospheric pressure;
DOI:10.1002/hc.20013

Reference yield:

: 80474-99-3
tetraethyl (aminomethylene)bis(phosphonate)

: 740083-66-3
tetraethyl N-[(3,4-dihydroxyphenylpropyl)amino]methylbisphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 71.7 percent / benzene / 4 h / Heating

2: 78.8 percent / H₂ / Pd/C / ethyl acetate / 4 h / 20 °C / atmospheric pressure

With hydrogen; palladium on activated charcoal; In ethyl acetate; benzene;
DOI:10.1002/hc.20013

Reference yield:

: (E)-3,4-bis(benzyloxy)cinnamaldehyde

: 740083-66-3
tetraethyl N-[(3,4-dihydroxyphenylpropyl)amino]methylbisphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 71.7 percent / benzene / 4 h / Heating

2: 78.8 percent / H₂ / Pd/C / ethyl acetate / 4 h / 20 °C / atmospheric pressure

With hydrogen; palladium on activated charcoal; In ethyl acetate; benzene;
DOI:10.1002/hc.20013