1-(3-Isopropyl-4-methyl-pent-4-enyl)-3-methoxymethoxymethyl-2-methyl-benzene

Base Information

Chemical Name:1-(3-Isopropyl-4-methyl-pent-4-enyl)-3-methoxymethoxymethyl-2-methyl-benzene
CAS No.:218765-83-4
Molecular Formula:C₁₉H₃₀O₂
Molecular Weight:290.446
Hs Code.:

Synonyms:1-(3-Isopropyl-4-methyl-pent-4-enyl)-3-methoxymethoxymethyl-2-methyl-benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3-Isopropyl-4-methyl-pent-4-enyl)-3-methoxymethoxymethyl-2-methyl-benzene

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Technology Process of 1-(3-Isopropyl-4-methyl-pent-4-enyl)-3-methoxymethoxymethyl-2-methyl-benzene

There total 9 articles about 1-(3-Isopropyl-4-methyl-pent-4-enyl)-3-methoxymethoxymethyl-2-methyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 218765-82-3
3-Isopropyl-1-(3-methoxymethoxymethyl-2-methyl-phenyl)-4-methyl-pent-4-en-1-one

: 218765-83-4
1-(3-Isopropyl-4-methyl-pent-4-enyl)-3-methoxymethoxymethyl-2-methyl-benzene

Guidance literature:: With potassium hydroxide; hydrazine; In diethylene glycol; at 118 - 232 ℃;
DOI:10.1016/S0040-4039(98)01965-0

Reference yield:

: 1975-50-4
2-methyl-3-nitrobenzic acid

: 218765-83-4
1-(3-Isopropyl-4-methyl-pent-4-enyl)-3-methoxymethoxymethyl-2-methyl-benzene

Guidance literature:: Multi-step reaction with 7 steps

1: H₂ / Pd/C / dimethylformamide / 2223.7 Torr

2: 1.) NaNO₂, HCl; 2.) KI / 1.) DMF

3: 83 percent / BH₃*SMe₂, B(OMe)3 / tetrahydrofuran / 20 °C

4: 97 percent / i-Pr₂NEt / CH₂Cl₂ / 0 - 20 °C

5: t-BuLi / tetrahydrofuran

6: TPAP, NMO / CH₂Cl₂ / 0 - 22 °C

7: 92 percent / H₂NNH₂, KOH / bis-(2-hydroxy-ethyl) ether / 118 - 232 °C

With hydrogenchloride; potassium hydroxide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; Trimethyl borate; dimethylsulfide borane complex; hydrogen; tert.-butyl lithium; N-ethyl-N,N-diisopropylamine; potassium iodide; hydrazine; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; diethylene glycol;
DOI:10.1016/S0040-4039(98)01965-0

Reference yield:

: 133232-56-1
3-iodo-2-methylbenzoic acid

: 218765-83-4
1-(3-Isopropyl-4-methyl-pent-4-enyl)-3-methoxymethoxymethyl-2-methyl-benzene

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / BH₃*SMe₂, B(OMe)3 / tetrahydrofuran / 20 °C

2: 97 percent / i-Pr₂NEt / CH₂Cl₂ / 0 - 20 °C

3: t-BuLi / tetrahydrofuran

4: TPAP, NMO / CH₂Cl₂ / 0 - 22 °C

5: 92 percent / H₂NNH₂, KOH / bis-(2-hydroxy-ethyl) ether / 118 - 232 °C

With potassium hydroxide; N-methyl-2-indolinone; tetrapropylammonium perruthennate; Trimethyl borate; dimethylsulfide borane complex; tert.-butyl lithium; N-ethyl-N,N-diisopropylamine; hydrazine; In tetrahydrofuran; dichloromethane; diethylene glycol;
DOI:10.1016/S0040-4039(98)01965-0