3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one hydrochloride

Base Information

Chemical Name:3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one hydrochloride
CAS No.:1620955-37-4
Molecular Formula:C₂₇H₂₄N₄O₃S*ClH
Molecular Weight:521.039
Hs Code.:

Synonyms:3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one hydrochloride

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Chemical Property of 3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one hydrochloride

Chemical Property:

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Technology Process of 3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one hydrochloride

There total 10 articles about 3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620951-89-4
3-(2-(4'-(4-((tetrahydro-2H-pyran-2-yl)oxy)butoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one

: 1620955-37-4
3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; methanol; dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 1620955-34-1
C₄₆H₄₄N₄O₆

: 1620955-37-4
3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane; dichloromethane; methanol / 2 h / 0 °C

With piperidine; hydrogenchloride; triethylamine; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1620955-35-2
C₃₁H₃₄N₄O₄

: 1620955-37-4
3-(2-(4'-(4-hydroxybutoxy)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridin-4-yl)-2-thioxoimidazolidin-4-one hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane; dichloromethane; methanol / 2 h / 0 °C

With hydrogenchloride; triethylamine; In 1,4-dioxane; methanol; dichloromethane;