Technology Process of C34H41Cl2N3O9S
There total 9 articles about C34H41Cl2N3O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 45 ℃;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C
2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C
3.1: methanol; chloroform / 2 h / 20 °C
4.1: potassium tert-butylate; methanol / toluene / 24 h / 20 °C
5.1: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 5 h / 20 °C
6.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1 h / 20 °C
7.1: N,N-dimethyl-formamide / 120 h / 100 °C
8.1: potassium carbonate / N,N-dimethyl-formamide / 45 °C
With
methanol; dmap; potassium tert-butylate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; chloroform; ethyl acetate; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C
2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C
3.1: methanol; chloroform / 2 h / 20 °C
4.1: potassium tert-butylate; methanol / toluene / 24 h / 20 °C
5.1: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 5 h / 20 °C
6.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 1 h / 20 °C
7.1: N,N-dimethyl-formamide / 120 h / 100 °C
8.1: potassium carbonate / N,N-dimethyl-formamide / 45 °C
With
methanol; dmap; potassium tert-butylate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; chloroform; ethyl acetate; N,N-dimethyl-formamide; toluene;