C₉H₁₁ClFN₃O₂S

Base Information

Chemical Name:C₉H₁₁ClFN₃O₂S
CAS No.:69202-53-5
Molecular Formula:C₉H₁₁ClFN₃O₂S
Molecular Weight:279.723
Hs Code.:

C<sub>9</sub>H<sub>11</sub>ClFN<sub>3</sub>O<sub>2</sub>S

Synonyms:C₉H₁₁ClFN₃O₂S

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Chemical Property of C₉H₁₁ClFN₃O₂S

Chemical Property:

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Technology Process of C₉H₁₁ClFN₃O₂S

There total 6 articles about C₉H₁₁ClFN₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 69156-32-7
C₉H₉ClFN₃O₄S

: 69202-53-5
C₉H₁₁ClFN₃O₂S

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; at 20 ℃; under 75.006 Torr;
DOI:10.1021/jm00362a017

Reference yield:

: 2106-02-7
2-chloro-4-fluoroaniline

: 69202-53-5
C₉H₁₁ClFN₃O₂S

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaNO₂, HCl, 2.) CuCl₂*2H₂O, HOAc, SO₂ / 1.) H₂O, 2.) H₂O, RT

2: 90 percent / NH₃ / Ambient temperature

3: 87 percent / dimethylformamide / 30 h / 60 °C

4: 94 percent / fuming sulfuric acid (20percent SO₂), fuming HNO₃ / 2 h / 55 °C

5: 90 percent / H₂ / 5percent Pd/C / tetrahydrofuran / 20 °C / 75.01 Torr

With hydrogenchloride; sulfuric acid; sulfur dioxide; sulfur trioxide; ammonia; hydrogen; nitric acid; acetic acid; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00362a017

Reference yield:

: 69156-31-6
C₉H₁₀ClFN₂O₂S

: 69202-53-5
C₉H₁₁ClFN₃O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / fuming sulfuric acid (20percent SO₂), fuming HNO₃ / 2 h / 55 °C

2: 90 percent / H₂ / 5percent Pd/C / tetrahydrofuran / 20 °C / 75.01 Torr

With sulfuric acid; sulfur trioxide; hydrogen; nitric acid; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jm00362a017