(R)-3-methyl-2-oxoimidazolidine-1,4-dicarboxylic acid 1-benzyl ester 4-tert-butyl ester

Base Information

Chemical Name:(R)-3-methyl-2-oxoimidazolidine-1,4-dicarboxylic acid 1-benzyl ester 4-tert-butyl ester
CAS No.:1426408-61-8
Molecular Formula:C₁₇H₂₂N₂O₅
Molecular Weight:334.372
Hs Code.:

Synonyms:(R)-3-methyl-2-oxoimidazolidine-1,4-dicarboxylic acid 1-benzyl ester 4-tert-butyl ester

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Chemical Property of (R)-3-methyl-2-oxoimidazolidine-1,4-dicarboxylic acid 1-benzyl ester 4-tert-butyl ester

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Technology Process of (R)-3-methyl-2-oxoimidazolidine-1,4-dicarboxylic acid 1-benzyl ester 4-tert-butyl ester

There total 2 articles about (R)-3-methyl-2-oxoimidazolidine-1,4-dicarboxylic acid 1-benzyl ester 4-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 352665-38-4
(R)-2-oxoimidazolidine-1,5-dicarboxylic acid 1-benzyl ester 5-tert-butyl ester

: 74-88-4
methyl iodide

: 1426408-61-8
(R)-3-methyl-2-oxoimidazolidine-1,4-dicarboxylic acid 1-benzyl ester 4-tert-butyl ester

Guidance literature:: (R)-2-oxoimidazolidine-1,5-dicarboxylic acid 1-benzyl ester 5-tert-butyl ester; With sodium hydride; In N,N-dimethyl-formamide; for 0.666667h; Cooling with ice;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Cooling with ice;

Reference yield:

: 634614-25-8
(R)-2-oxoimidazolidine-1,5-dicarboxylic acid 1-benzyl ester

: 1426408-61-8
(R)-3-methyl-2-oxoimidazolidine-1,4-dicarboxylic acid 1-benzyl ester 4-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; trichlorophosphate / water; chloroform / 5 h / 20 °C / Cooling with ice

2.1: sodium hydride / N,N-dimethyl-formamide / 0.67 h / Cooling with ice

2.2: 4 h / 20 °C / Cooling with ice

With pyridine; sodium hydride; trichlorophosphate; In chloroform; water; N,N-dimethyl-formamide;

Reference yield:

: 1426408-61-8
(R)-3-methyl-2-oxoimidazolidine-1,4-dicarboxylic acid 1-benzyl ester 4-tert-butyl ester

: 1426402-15-4
((R)-3-methyl-2-oxoimidazolidine-4-carboxylic acid [1-phenyl-5-(3-propylphenyl)-1H-pyrazol-3-yl]amide)

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 15 h / 20 °C / 760.05 Torr

2: trifluoroacetic acid / chloroform / 3 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxybenzotriazol-hydrate / N,N-dimethyl-formamide / 2 h / 20 °C

With palladium 10% on activated carbon; hydrogen; 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In methanol; chloroform; N,N-dimethyl-formamide;