5-chloro-6-(2,6-dichlorophenyl)-3-(1-methyl-2-oxopropylamino)-2H-1,4-oxazin-2-one

Base Information

Chemical Name:5-chloro-6-(2,6-dichlorophenyl)-3-(1-methyl-2-oxopropylamino)-2H-1,4-oxazin-2-one
CAS No.:225108-63-4
Molecular Formula:C₁₄H₁₁Cl₃N₂O₃
Molecular Weight:361.612
Hs Code.:

Synonyms:5-chloro-6-(2,6-dichlorophenyl)-3-(1-methyl-2-oxopropylamino)-2H-1,4-oxazin-2-one

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Chemical Property of 5-chloro-6-(2,6-dichlorophenyl)-3-(1-methyl-2-oxopropylamino)-2H-1,4-oxazin-2-one

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Technology Process of 5-chloro-6-(2,6-dichlorophenyl)-3-(1-methyl-2-oxopropylamino)-2H-1,4-oxazin-2-one

There total 1 articles about 5-chloro-6-(2,6-dichlorophenyl)-3-(1-methyl-2-oxopropylamino)-2H-1,4-oxazin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 21419-24-9
3-Amino-2-butanone hydrochloride

: 160921-62-0
3,5-Dichloro-6-(2,6-dichloro-phenyl)-[1,4]oxazin-2-one

: 225108-64-5
3-(2,2-dimethoxyethylamino)-2H-1,4-benzoxazin-2-one

: 225108-63-4
5-chloro-6-(2,6-dichlorophenyl)-3-(1-methyl-2-oxopropylamino)-2H-1,4-oxazin-2-one

Guidance literature:: With triethylamine; In ethyl acetate; for 2h; Heating;
DOI:10.1016/S0040-4020(99)00087-3

Reference yield: 90.0%

: 225108-63-4
5-chloro-6-(2,6-dichlorophenyl)-3-(1-methyl-2-oxopropylamino)-2H-1,4-oxazin-2-one

: 5-chloro-6-(2,6-dichlorophenyl)-2,3-dimethyl-8H-imiddazo<2,1-c><1,4>oxazin-8

Guidance literature:: With acetic anhydride; trifluoroacetic acid; at 60 ℃; for 4h;
DOI:10.1016/S0040-4020(99)00087-3

Reference yield:

: 225108-63-4
5-chloro-6-(2,6-dichlorophenyl)-3-(1-methyl-2-oxopropylamino)-2H-1,4-oxazin-2-one

: (+/-)-1-<1-chloro-2-(2,6-dichlorophenyl)-2-oxoethyl>-4,5-dimethyl-N,N-diethyl-1H-imidazole-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / acetic anhydride, trifluoroacetic acid / 4 h / 60 °C

2: 87 percent / 0.75 h / Ambient temperature

With acetic anhydride; trifluoroacetic acid;
DOI:10.1016/S0040-4020(99)00087-3