Technology Process of C24H35NO5
There total 8 articles about C24H35NO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: ethanol; sodium / tetrahydrofuran / 20 °C
2: sodium chloride / dimethyl sulfoxide / 150 °C
3: trimethylaluminum; ammonium chloride / toluene / 40 °C
4: sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / 150 °C
5: pyridinium p-toluenesulfonate / methanol / 20 °C
6: dmap; triethylamine / dichloromethane / 20 °C
7: lithium diisopropyl amide / tetrahydrofuran / -78 °C
With
dmap; ethanol; trimethylaluminum; sodium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine; sodium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1016/j.bmcl.2012.05.065
- Guidance literature:
-
Multi-step reaction with 9 steps
1: magnesium / tetrahydrofuran / 20 °C
2: 3,3-dimethyldioxirane; sodium hydrogencarbonate / water; acetone / 20 °C
3: ethanol; sodium / tetrahydrofuran / 20 °C
4: sodium chloride / dimethyl sulfoxide / 150 °C
5: trimethylaluminum; ammonium chloride / toluene / 40 °C
6: sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / 150 °C
7: pyridinium p-toluenesulfonate / methanol / 20 °C
8: dmap; triethylamine / dichloromethane / 20 °C
9: lithium diisopropyl amide / tetrahydrofuran / -78 °C
With
dmap; ethanol; trimethylaluminum; sodium; 3,3-dimethyldioxirane; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; ammonium chloride; magnesium; triethylamine; N-ethyl-N,N-diisopropylamine; sodium chloride; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; acetone; toluene;
DOI:10.1016/j.bmcl.2012.05.065