N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine isopenylamide

Base Information

Chemical Name:N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine isopenylamide
CAS No.:96866-23-8
Molecular Formula:C₂₅H₃₁N₃O₄
Molecular Weight:437.539
Hs Code.:

Synonyms:N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine isopenylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine isopenylamide

Chemical Property:

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Technology Process of N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine isopenylamide

There total 3 articles about N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine isopenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 96866-22-7
N-(3-carboxy-2-benzylidene-1-oxopropyl)glycine isopentylamide

: 96866-23-8
N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine isopenylamide

Guidance literature:: With benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; chloroform; Ambient temperature;
DOI:10.1021/jm00147a007

Reference yield:

: 87439-00-7
3-(ethoxycarbonyl)-2-benzylidenepropanoic acid

: 96866-23-8
N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine isopenylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

2: 76 percent / 1 N aq. NaOH / ethanol / 4 h / Ambient temperature

3: 81 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jm00147a007

Reference yield:

: 96866-21-6
N-<3-(ethoxycarbonyl)-2-benzylidene-1-oxopropyl>glycine isopentylamide

: 96866-23-8
N-<3-<<(benzyloxy)amino>carbonyl>-2-benzylidene-1-oxopropyl>glycine isopenylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / 1 N aq. NaOH / ethanol / 4 h / Ambient temperature

2: 81 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jm00147a007