3-benzyloxy-N-(4'-bromobutyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

Base Information

Chemical Name:3-benzyloxy-N-(4'-bromobutyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide
CAS No.:415974-52-6
Molecular Formula:C₂₉H₃₄BrNO₃
Molecular Weight:524.498
Hs Code.:

3-benzyloxy-N-(4'-bromobutyl)-16,17-seco-estra-1,3,5<sup>(10)</sup>-triene-16,17-imide

Synonyms:3-benzyloxy-N-(4'-bromobutyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

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Chemical Property of 3-benzyloxy-N-(4'-bromobutyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

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Technology Process of 3-benzyloxy-N-(4'-bromobutyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

There total 2 articles about 3-benzyloxy-N-(4'-bromobutyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 415974-45-7
3-benzyloxy-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

: 415974-52-6
3-benzyloxy-N-(4'-bromobutyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

Guidance literature:: 3-benzyloxy-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide; With sodium hydride; In N,N-dimethyl-formamide;

4'-bromobutyl halide; In N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(03)00042-7

Reference yield:

: 415974-44-6
3-benzyloxy-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-dioic acid

: 415974-52-6
3-benzyloxy-N-(4'-bromobutyl)-16,17-seco-estra-1,3,5⁽¹⁰⁾-triene-16,17-imide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 89 percent / urea / 0.75 h / 180 °C

2.1: NaH / dimethylformamide

2.2: 84 percent / dimethylformamide

With sodium hydride; urea; In N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(03)00042-7