Technology Process of C20H23(2)HO3
There total 7 articles about C20H23(2)HO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium borodeuteride;
In
methanol;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 23 percent / potassium carbonate, potassium iodide / acetone / 65 h / Heating
2: 91 percent / H2 / Lindlar catalyst / ethyl acetate / 20 °C
3: 86 percent / 0.1 h / 135 °C
4: 83 percent / potassium carbonate, potassium iodide / acetone / 16 h / Heating
5: 90 percent / sodium borodeuteride / methanol / 1 h / 20 °C
With
sodium borodeuteride; hydrogen; potassium carbonate; potassium iodide;
Lindlar's catalyst;
In
methanol; ethyl acetate; acetone;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 91 percent / H2 / Lindlar catalyst / ethyl acetate / 20 °C
2: 86 percent / 0.1 h / 135 °C
3: 83 percent / potassium carbonate, potassium iodide / acetone / 16 h / Heating
4: 90 percent / sodium borodeuteride / methanol / 1 h / 20 °C
With
sodium borodeuteride; hydrogen; potassium carbonate; potassium iodide;
Lindlar's catalyst;
In
methanol; ethyl acetate; acetone;