5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine-10,11-dicarbonitrile

Base Information

• Chemical Name: 5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine-10,11-dicarbonitrile
• CAS No.: 1011490-90-6
• Molecular Formula: C₄₁H₃₈N₄O₆S₄
• Molecular Weight: 811.04

Synonyms:5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine-10,11-dicarbonitrile

Chemical Property of 5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine-10,11-dicarbonitrile

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Technology Process of 5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine-10,11-dicarbonitrile

There total 1 articles about 5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine-10,11-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

10,11-dibromo-5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine + copper(I) cyanide (544-92-3) → 5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine-10,11-dicarbonitrile (1011490-90-6)

Guidance literature:

In pyridine; N,N-dimethyl-formamide; for 48h; Heating;

DOI:10.1016/j.jorganchem.2007.11.022

Reference yield: 44.0%

5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine-10,11-dicarbonitrile (1011490-90-6) → C164H152N16O24S16(2-)*Co(2+)

Guidance literature:

With CoCl₂; In quinoline; at 220 ℃; for 0.25h; microwave irradiation;

DOI:10.1016/j.jorganchem.2007.11.022

Reference yield: 41.0%

5,16-bis[(4-methylphenyl)sulfonyl]-6,7,15,16,23,24-hexahydro-5H,14H,22H-tribenzo[b,h,o][1,4,10,14,7,17]dioxadithiadiazacyclononadecine-10,11-dicarbonitrile (1011490-90-6) → C164H154N16O24S16

Guidance literature:

In quinoline; at 220 ℃; for 0.25h; microwave irradiation;

DOI:10.1016/j.jorganchem.2007.11.022

upstream raw materials:

copper(I) cyanide

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