{4-[2-(4-nitrophenyl)-2-oxoethyl]-4H-[1,2,4]triazol-1-io}(phenyl)(2,4,6-trinitrophenyl)methanide

Base Information

Chemical Name:{4-[2-(4-nitrophenyl)-2-oxoethyl]-4H-[1,2,4]triazol-1-io}(phenyl)(2,4,6-trinitrophenyl)methanide
CAS No.:349102-51-8
Molecular Formula:C₂₃H₁₅N₇O₉
Molecular Weight:533.414
Hs Code.:

Synonyms:{4-[2-(4-nitrophenyl)-2-oxoethyl]-4H-[1,2,4]triazol-1-io}(phenyl)(2,4,6-trinitrophenyl)methanide

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Chemical Property of {4-[2-(4-nitrophenyl)-2-oxoethyl]-4H-[1,2,4]triazol-1-io}(phenyl)(2,4,6-trinitrophenyl)methanide

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Technology Process of {4-[2-(4-nitrophenyl)-2-oxoethyl]-4H-[1,2,4]triazol-1-io}(phenyl)(2,4,6-trinitrophenyl)methanide

There total 3 articles about {4-[2-(4-nitrophenyl)-2-oxoethyl]-4H-[1,2,4]triazol-1-io}(phenyl)(2,4,6-trinitrophenyl)methanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88-88-0
2,4,6-trinitrochlorobenzene

: 1-benzyl-4-(2-(4-nitrophenyl)-2-oxoethyl)-1H-1,2,4-triazol-4-ium bromide

: 349102-48-3
(1-benzyl-1H-[1,2,4]triazol-4-io)(4-nitrobenzoyl)(2,4,6-trinitrophenyl)methanide

: 349102-51-8
{4-[2-(4-nitrophenyl)-2-oxoethyl]-4H-[1,2,4]triazol-1-io}(phenyl)(2,4,6-trinitrophenyl)methanide

Guidance literature:: With triethylamine; In chloroform; at 0 - 20 ℃; for 3h; Title compound not separated from byproducts;
DOI:10.1002/1099-0690(200104)2001:7<1407::aid-ejoc1407>3.0.co;2-n

Reference yield:

: 6085-94-5
1-benzyl-1,2,4-triazole

: 349102-51-8
{4-[2-(4-nitrophenyl)-2-oxoethyl]-4H-[1,2,4]triazol-1-io}(phenyl)(2,4,6-trinitrophenyl)methanide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / acetone / 8 h / Heating

2: Et₃N / CHCl₃ / 3 h / 0 - 20 °C

With triethylamine; In chloroform; acetone;
DOI:10.1002/1099-0690(200104)2001:7<1407::aid-ejoc1407>3.0.co;2-n

Reference yield:

: 100-39-0
benzyl bromide

: 349102-51-8
{4-[2-(4-nitrophenyl)-2-oxoethyl]-4H-[1,2,4]triazol-1-io}(phenyl)(2,4,6-trinitrophenyl)methanide

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / ethanol

2: 75 percent / acetone / 8 h / Heating

3: Et₃N / CHCl₃ / 3 h / 0 - 20 °C

With sodium hydride; triethylamine; In ethanol; chloroform; acetone;
DOI:10.1002/1099-0690(200104)2001:7<1407::aid-ejoc1407>3.0.co;2-n