C₂₇H₃₈O₃Si

Base Information

Chemical Name:C₂₇H₃₈O₃Si
CAS No.:1404304-66-0
Molecular Formula:C₂₇H₃₈O₃Si
Molecular Weight:438.682
Hs Code.:

C<sub>27</sub>H<sub>38</sub>O<sub>3</sub>Si

Synonyms:C₂₇H₃₈O₃Si

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Chemical Property of C₂₇H₃₈O₃Si

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Technology Process of C₂₇H₃₈O₃Si

There total 5 articles about C₂₇H₃₈O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1404304-65-9
C₂₆H₃₆O₂Si

: 1404304-66-0
C₂₇H₃₈O₃Si

Guidance literature:: C₂₆H₃₆O₂Si; With n-butyllithium; In diethyl ether; hexane; at -78 - -15 ℃; for 1h; Inert atmosphere;

formaldehyd; In diethyl ether; hexane; for 3.5h; Inert atmosphere; Reflux;
DOI:10.1021/ol302409g

Reference yield:

: 33467-76-4
(E)-hept-2-en-1-ol

: 1404304-66-0
C₂₇H₃₈O₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: triphenylphosphine; tetrachloromethane / 24 h / 80 °C / Inert atmosphere

2.1: (DHQD)_2PHAL; methanesulfonamide; potassium osmate(VI) dihydrate; potassium hexacyanoferrate(III); potassium carbonate; sodium hydrogencarbonate / tert-butyl alcohol; water / 4 h / 0 °C / Inert atmosphere

3.1: sodium hydroxide / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

4.1: 1H-imidazole / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

5.1: mercury dichloride; iodine; magnesium / diethyl ether; toluene / 1 h / 0 - 20 °C / Inert atmosphere

5.2: 1.5 h / -78 - 20 °C / Inert atmosphere

6.1: n-butyllithium / diethyl ether; hexane / 1 h / -78 - -15 °C / Inert atmosphere

6.2: 3.5 h / Inert atmosphere; Reflux

With (DHQD)_2PHAL; 1H-imidazole; tetrachloromethane; potassium osmate(VI) dihydrate; n-butyllithium; methanesulfonamide; iodine; sodium hydrogencarbonate; potassium carbonate; magnesium; triphenylphosphine; mercury dichloride; sodium hydroxide; potassium hexacyanoferrate(III); In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; toluene; tert-butyl alcohol; 2.1: |Sharpless Dihydroxylation;
DOI:10.1021/ol302409g

Reference yield:

: 1404304-64-8
C₂₃H₃₂O₂Si

: 1404304-66-0
C₂₇H₃₈O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: mercury dichloride; iodine; magnesium / diethyl ether; toluene / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 1.5 h / -78 - 20 °C / Inert atmosphere

2.1: n-butyllithium / diethyl ether; hexane / 1 h / -78 - -15 °C / Inert atmosphere

2.2: 3.5 h / Inert atmosphere; Reflux

With n-butyllithium; iodine; magnesium; mercury dichloride; In diethyl ether; hexane; toluene;
DOI:10.1021/ol302409g