C₁₆H₂₂BrNO₄

Base Information

• Chemical Name: C₁₆H₂₂BrNO₄
• CAS No.: 1376600-38-2
• Molecular Formula: C₁₆H₂₂BrNO₄
• Molecular Weight: 372.259
• Mol file: 1376600-38-2.mol

Synonyms:C₁₆H₂₂BrNO₄

Chemical Property of C₁₆H₂₂BrNO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₂₂BrNO₄

There total 1 articles about C₁₆H₂₂BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.2%

N-(Benzyloxycarbonyloxy)succinimide (13139-17-8) + (S)-2-amino-8-bromooctanoic acid → C16H22BrNO4 (1376600-38-2)

Guidance literature:

With sodium carbonate; In water; acetone; for 5h;

DOI:10.1016/j.ejmech.2012.03.009

Reference yield: 90.2%

C16H22BrNO4 (1376600-38-2) + tert-butyl alcohol (75-65-0) → C20H30BrNO4 (1376600-41-7)

Guidance literature:

With dmap; di-tert-butyl dicarbonate;

DOI:10.1016/j.ejmech.2012.03.009

Reference yield:

C16H22BrNO4 (1376600-38-2) → C34H36N2O4S2 (1376600-12-2)

Guidance literature:

Multi-step reaction with 5 steps

1: dmap; di-tert-butyl dicarbonate

2: N,N-dimethyl-formamide / 5 h

3: methanol; nitromethane; N,N-dimethyl-formamide / 6 h / Inert atmosphere

4: trifluoroacetic acid / 2 h / 0 °C

5: dmap; dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 8 h

With dmap; di-tert-butyl dicarbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In methanol; nitromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2012.03.009

upstream raw materials:

N-(Benzyloxycarbonyloxy)succinimide

Downstream raw materials:

C₃₁H₃₃N₃O₃S₂

C₂₇H₃₇N₃O₃S₂

C₃₀H₃₂N₄O₃S₃

C₃₃H₃₅N₃O₃S₂