C₄₅H₆₀N₂O₁₂S

Base Information

Chemical Name:C₄₅H₆₀N₂O₁₂S
CAS No.:1422364-39-3
Molecular Formula:C₄₅H₆₀N₂O₁₂S
Molecular Weight:853.044
Hs Code.:

C<sub>45</sub>H<sub>60</sub>N<sub>2</sub>O<sub>12</sub>S

Synonyms:C₄₅H₆₀N₂O₁₂S

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Chemical Property of C₄₅H₆₀N₂O₁₂S

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Technology Process of C₄₅H₆₀N₂O₁₂S

There total 7 articles about C₄₅H₆₀N₂O₁₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.9%

: 1429398-18-4
C₄₇H₆₂N₂O₁₃S

: 1422364-39-3
C₄₅H₆₀N₂O₁₂S

Guidance literature:: With methanol; at 65 ℃; for 3h;
DOI:10.1016/j.ejmech.2012.10.054

Reference yield:

: 561327-03-5
(E)-5-O-desosaminyl-6-O-methylerythronolide A 9-oxime

: 1422364-39-3
C₄₅H₆₀N₂O₁₂S

Guidance literature:: Multi-step reaction with 6 steps

1.1: dichloromethane / 1 h / 20 °C

2.1: potassium tert-butylate / N,N-dimethyl-formamide / 0.17 h

2.2: 1 h / 20 °C

3.1: pyridine / dichloromethane / 16 h / -5 - 20 °C

4.1: N-chloro-succinimide; dimethylsulfide / dichloromethane

4.2: 1 h / -5 °C

5.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) iodide / acetonitrile / 3 h / 80 °C / Sealed tube

6.1: methanol / 3 h / 65 °C

With pyridine; methanol; bis-triphenylphosphine-palladium(II) chloride; N-chloro-succinimide; copper(l) iodide; dimethylsulfide; potassium tert-butylate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; acetonitrile; 5.1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.ejmech.2012.10.054

Reference yield:

: 1422364-32-6
C₃₆H₅₆N₂O₁₂

: 1422364-39-3
C₄₅H₆₀N₂O₁₂S

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) iodide / acetonitrile / 3 h / 80 °C / Sealed tube

2: methanol / 3 h / 65 °C

With methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In acetonitrile; 1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.ejmech.2012.10.054