ethyl 5-(4'-methylpent-3'-en-1'-yl)-2-phenyl-1-pyrroline-5-carboxylate 1-oxide

Base Information

Chemical Name:ethyl 5-(4'-methylpent-3'-en-1'-yl)-2-phenyl-1-pyrroline-5-carboxylate 1-oxide
CAS No.:212265-34-4
Molecular Formula:C₁₉H₂₅NO₃
Molecular Weight:315.412
Hs Code.:

Synonyms:ethyl 5-(4'-methylpent-3'-en-1'-yl)-2-phenyl-1-pyrroline-5-carboxylate 1-oxide

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Chemical Property of ethyl 5-(4'-methylpent-3'-en-1'-yl)-2-phenyl-1-pyrroline-5-carboxylate 1-oxide

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Technology Process of ethyl 5-(4'-methylpent-3'-en-1'-yl)-2-phenyl-1-pyrroline-5-carboxylate 1-oxide

There total 1 articles about ethyl 5-(4'-methylpent-3'-en-1'-yl)-2-phenyl-1-pyrroline-5-carboxylate 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 212265-33-3
ethyl 2-phenyl-1-pyrroline-5-carboxylate 1-oxide

: 212265-34-4
ethyl 5-(4'-methylpent-3'-en-1'-yl)-2-phenyl-1-pyrroline-5-carboxylate 1-oxide

Guidance literature:: ethyl 2-phenyl-1-pyrroline-5-carboxylate 1-oxide; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h;

Me₂C=CH(CH₂)2X, X = halide; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1055/s-2006-942380

Reference yield: 63.0%

: 212265-34-4
ethyl 5-(4'-methylpent-3'-en-1'-yl)-2-phenyl-1-pyrroline-5-carboxylate 1-oxide

: ethyl cis-2-(4'-methylpent-3'-en-1'-yl)-5-phenyl-6-oxa-1-azabicyclo[3.1.0]hexane-2-carboxylate

: ethyl trans-2-(4'-methylpent-3'-en-1'-yl)-5-phenyl-6-oxa-1-azabicyclo[3.1.0]hexane-2-carboxylate

Guidance literature:: In benzene; for 16h; UV-irradiation;
DOI:10.1055/s-2006-942380

Reference yield:

: 212265-34-4
ethyl 5-(4'-methylpent-3'-en-1'-yl)-2-phenyl-1-pyrroline-5-carboxylate 1-oxide

: ethyl 6,6-dimethyl-2-(3'-phenyl-3'-oxoprop-1'-yl)-1-azabicyclo[3.1.0]hexane-2-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 14 percent / benzene / 16 h / UV-irradiation

2: 87 percent / [Cu(PPh₃)Cl]4 / tetrahydrofuran / Heating

3: 31 percent / magnesium monoperoxyphthalate / methanol / 0.5 h / 20 °C

4: 89 percent / [Cu(PPh₃)Cl]4 / tetrahydrofuran / Heating

With tetrakis[chloro(triphenylphosphine)copper(I)]; magnesium monoperoxyphthalate hexahydrate; In tetrahydrofuran; methanol; benzene;
DOI:10.1055/s-2006-942380