Docosa-10,12-diynedioic acid bis-{(S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl} ester

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Chemical Name:Docosa-10,12-diynedioic acid bis-{(S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl} ester
CAS No.:183145-15-5
Molecular Formula:C₆₄H₈₂O₁₂
Molecular Weight:1043.35
Hs Code.:

Synonyms:Docosa-10,12-diynedioic acid bis-{(S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl} ester

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Chemical Property of Docosa-10,12-diynedioic acid bis-{(S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl} ester

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Technology Process of Docosa-10,12-diynedioic acid bis-{(S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl} ester

There total 4 articles about Docosa-10,12-diynedioic acid bis-{(S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 183145-05-3
Undec-10-ynoic acid (S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl ester

: 183145-15-5
Docosa-10,12-diynedioic acid bis-{(S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl} ester

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; oxygen; copper(l) chloride; In xylene; at 140 - 150 ℃; for 0.75h;
DOI:10.1021/jo9605455

Reference yield:

: 2777-65-3
undec-10-ynoic acid

: 183145-15-5
Docosa-10,12-diynedioic acid bis-{(S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl} ester

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / DMAP, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

2: 76 percent / DMAP, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

3: 84 percent / O₂, CuCl, TMEDA / xylene / 0.75 h / 140 - 150 °C

With dmap; N,N,N,N,-tetramethylethylenediamine; oxygen; dicyclohexyl-carbodiimide; copper(l) chloride; In dichloromethane; xylene;
DOI:10.1021/jo9605455

Reference yield:

: 56552-80-8
(R)-3-benzyloxy-1,2-propanediol

: 183145-15-5
Docosa-10,12-diynedioic acid bis-{(S)-3-benzyloxy-2-[4-(4-methoxy-phenyl)-butyryloxy]-propyl} ester

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / DMAP, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

2: 76 percent / DMAP, 1,3-dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

3: 84 percent / O₂, CuCl, TMEDA / xylene / 0.75 h / 140 - 150 °C

With dmap; N,N,N,N,-tetramethylethylenediamine; oxygen; dicyclohexyl-carbodiimide; copper(l) chloride; In dichloromethane; xylene;
DOI:10.1021/jo9605455