methyl onate

Base Information

• Chemical Name: methyl onate
• CAS No.: 94528-58-2
• Molecular Formula: C₄₄H₄₂O₁₆
• Molecular Weight: 826.808
• Mol file: 94528-58-2.mol

Synonyms:methyl onate

Chemical Property of methyl onate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl onate

There total 2 articles about methyl onate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

methyl (methyl 8-O-benzyl-4,5-O-carbonyl-3-deoxy-β-D-manno-2-octulopyranosid)onate (94528-57-1) + 2,3,5-tri-O-benzoyl-D-ribofuranosyl bromide (22860-91-9) → methyl onate (94528-58-2)

Guidance literature:

With calcium sulfate; silver trifluoromethanesulfonate; In dichloromethane; at -25 ℃; for 0.25h;

DOI:10.1016/0008-6215(84)85223-4

Reference yield: 66.0%

methyl (methyl 8-O-benzyl-4,5-O-carbonyl-3-deoxy-α-D-manno-2-octulopyranosid)onate (93215-25-9) + 2,3,5-tri-O-benzoyl-D-ribofuranosyl bromide (22860-91-9) → methyl onate (94528-58-2)

Guidance literature:

With calcium sulfate; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; for 0.333333h;

DOI:10.1016/0008-6215(85)90002-3

Reference yield: 100.0%

methyl onate (94528-58-2) → methyl onate (93215-09-9)

Guidance literature:

With hydrogen; trimethyleneglycol; In methanol; ethyl acetate; for 48h; under 760 Torr;

DOI:10.1016/0008-6215(85)90002-3

upstream raw materials:

methyl (methyl 8-O-benzyl-4,5-O-carbonyl-3-deoxy-β-D-manno-2-octulopyranosid)onate

2,3,5-tri-O-benzoyl-D-ribofuranosyl bromide

methyl (methyl 8-O-benzyl-4,5-O-carbonyl-3-deoxy-α-D-manno-2-octulopyranosid)onate

Downstream raw materials:

methyl onate

methyl onate