trichloro[N-(biphenyl-2-yl)-N'-methyl-N'-oxybenzamidinato](tetrahydrofuran)zirconium(IV)

Base Information

Chemical Name:trichloro[N-(biphenyl-2-yl)-N'-methyl-N'-oxybenzamidinato](tetrahydrofuran)zirconium(IV)
CAS No.:582315-26-2
Molecular Formula:C₂₄H₂₅Cl₃N₂O₂Zr
Molecular Weight:571.058
Hs Code.:

Synonyms:trichloro[N-(biphenyl-2-yl)-N'-methyl-N'-oxybenzamidinato](tetrahydrofuran)zirconium(IV)

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Chemical Property of trichloro[N-(biphenyl-2-yl)-N'-methyl-N'-oxybenzamidinato](tetrahydrofuran)zirconium(IV)

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Technology Process of trichloro[N-(biphenyl-2-yl)-N'-methyl-N'-oxybenzamidinato](tetrahydrofuran)zirconium(IV)

There total 1 articles about trichloro[N-(biphenyl-2-yl)-N'-methyl-N'-oxybenzamidinato](tetrahydrofuran)zirconium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 10026-11-6
zirconium(IV) chloride

: 582315-20-6
N-(biphenyl-2-yl)-N'-hydroxy-N'-methylbenzamidine

: 582315-26-2
trichloro[N-(biphenyl-2-yl)-N'-methyl-N'-oxybenzamidinato](tetrahydrofuran)zirconium(IV)

Guidance literature:: With n-butyllithium; In tetrahydrofuran; pentane; byproducts: LiCl; Ar, to a soln. of amidino compd. (THF) added a soln. of Li compd. (pentane) at -80°C, stirred for 1 h, ZrCl4 (1.2 equiv.) added, stirred without cooling overnight; volatiles removed (vac.), residue dissolved (CH2Cl2), filtered, solvent removed (vac.), triturated (hexane), solvent removed, ppt. dried (vac.);elem. anal.;
DOI:10.1002/ejic.200300405