N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline

Base Information

Chemical Name:N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline
CAS No.:908014-88-0
Molecular Formula:C₆₆H₆₁N₃O₅
Molecular Weight:976.227
Hs Code.:

N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline

Synonyms:N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline

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Chemical Property of N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline

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Technology Process of N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline

There total 6 articles about N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 876732-76-2
N-(4-methoxyphenyl)-N-(3-methyl-4-vinylphenyl)-N-(4-vinylphenyl)amine

: N,N-bis(4-methoxyphenyl)-3-bromo-4-methylaniline

: 908014-88-0
N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline

Guidance literature:: With triethylamine; tris-(o-tolyl)phosphine; lithium chloride; palladium diacetate; In N,N-dimethyl-formamide; at 100 ℃; for 24h;
DOI:10.1246/bcsj.79.953

Reference yield:

: 908014-90-4
4-[N-(4-formylphenyl)-N-(4-methoxyphenyl)amino]-2-methylbenzaldehyde

: 908014-88-0
N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butlyllithium / tetrahydrofuran; hexane / 0.5 h

1.2: 67 percent / tetrahydrofuran; hexane / 19 h

2.1: 9 percent / tri-o-tolylphosphine; lithium chloride; triethylamine / palladium(II) acetate / dimethylformamide / 24 h / 100 °C

With n-butyllithium; triethylamine; tris-(o-tolyl)phosphine; lithium chloride; palladium diacetate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.79.953

Reference yield:

: 107816-54-6
4-[N-(4-methoxyphenyl)amino]benzaldehyde

: 908014-88-0
N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}-3-methylphenyl)-N-(4-{5-[N,N-bis(4-methoxyphenyl)amino]-2-methylstyryl}phenyl)-4-methoxyaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: 43 percent / 2,2'-bis(diphenylphosphino)-1,1'-binaphthalene; Cs₂CO₃ / [Pd₂(dibenzylideneacetone)3] / toluene / 72 h / 100 °C

2.1: n-butlyllithium / tetrahydrofuran; hexane / 0.5 h

2.2: 67 percent / tetrahydrofuran; hexane / 19 h

3.1: 9 percent / tri-o-tolylphosphine; lithium chloride; triethylamine / palladium(II) acetate / dimethylformamide / 24 h / 100 °C

With n-butyllithium; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triethylamine; tris-(o-tolyl)phosphine; lithium chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; toluene;
DOI:10.1246/bcsj.79.953