4-[N-(4-methoxyphenyl)amino]benzaldehyde

Base Information

Chemical Name:4-[N-(4-methoxyphenyl)amino]benzaldehyde
CAS No.:107816-54-6
Molecular Formula:C₁₄H₁₃NO₂
Molecular Weight:227.263
Hs Code.:

Synonyms:4-[N-(4-methoxyphenyl)amino]benzaldehyde

Suppliers and Price of 4-[N-(4-methoxyphenyl)amino]benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-[N-(4-methoxyphenyl)amino]benzaldehyde

Chemical Property:

Melting Point:113 °C(Solv: hexane (110-54-3); chloroform (67-66-3))
Boiling Point:396.6±27.0 °C(Predicted)
Density:1.188±0.06 g/cm3(Predicted)

Purity/Quality:: 95% ^*data from raw suppliers

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Technology Process of 4-[N-(4-methoxyphenyl)amino]benzaldehyde

There total 13 articles about 4-[N-(4-methoxyphenyl)amino]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 104-94-9
4-methoxy-aniline

: 107816-54-6
4-[N-(4-methoxyphenyl)amino]benzaldehyde

Guidance literature:: 4-hydroxy-benzaldehyde; 4-methoxy-aniline; With caesium carbonate; chloroacetyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

In N,N-dimethyl-formamide; at 150 ℃; Microwave irradiation;
DOI:10.3998/ark.5550190.0012.a10

Reference yield: 67.0%

: 104-94-9
4-methoxy-aniline

: 1122-91-4
4-bromo-benzaldehyde

: 107816-54-6
4-[N-(4-methoxyphenyl)amino]benzaldehyde

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 100 ℃; for 16h;
DOI:10.1021/ja0569611

Reference yield: 67.0%

: 100-17-4
para-methoxynitrobenzene

: 1122-91-4
4-bromo-benzaldehyde

: 107816-54-6
4-[N-(4-methoxyphenyl)amino]benzaldehyde

Guidance literature:: With (4,4′-di-tert-butyl-2,2′-dipyridyl)Ni(o-tolyl)(Br); N-ethyl-N,N-diisopropylamine; In toluene; at 70 ℃; for 12h; Molecular sieve; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1002/anie.202012877