(tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

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Chemical Name:(tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc
CAS No.:573658-43-2
Molecular Formula:C₆₇H₇₂N₄O₁₂SiZn
Molecular Weight:1218.8
Hs Code.:

(tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

Synonyms:(tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

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Chemical Property of (tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

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Technology Process of (tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

There total 2 articles about (tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoate

: 5970-45-6
zinc(II) acetate dihydrate

: 573658-43-2
(tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

Guidance literature:: In methanol; chloroform; (N2); Zn salt added to a soln. of ligand, stirred for 16 h at 20°C; evapd. (vac.), CH2Cl2 added, the org. phase washed (H2O), dried (MgSO4),evapd. (vac.); elem. anal.;
DOI:10.1002/hlca.200490288

Reference yield:

: 573658-50-1
(tetraethyl 4,4',4'',4'''-[[10-(2-bromophenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

: 1066-54-2
trimethylsilylacetylene

: 573658-43-2
(tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

Guidance literature:: With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In toluene; (N2); for 16 h at 90°C;
DOI:10.1002/hlca.200490288

Reference yield: 99.0%

: 573658-43-2
(tetraethyl 4,4',4'',4'''-[[10-(2-[(trimethylsilyl)ethynyl]phenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

: 849726-33-6
(tetraethyl 4,4',4'',4'''-[[10-(2-ethynylphenyl)porphyrin-5,15-diyl-κN(21),κN(22),κN(23),κN(24)]bis[benzene-2,1,3-triylbis(oxy)]]tetrabutanoato(2-))zinc

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; (N2); Bu4NF in THF added to a soln. of Zn complex, stirred for 15 min at20°C; H2O added, extd. (CH2Cl2), the combined org. layers dried (MgSO4), evapd. (vac.);
DOI:10.1002/hlca.200490288