2-chloro-N-(5-chloro-2-hydroxyphenyl)acetamide

Base Information

• Chemical Name: 2-chloro-N-(5-chloro-2-hydroxyphenyl)acetamide
• CAS No.: 35588-38-6
• Molecular Formula: C₈H₇Cl₂NO₂
• Molecular Weight: 220.055
• DSSTox Substance ID: DTXSID301248640

Synonyms:2-chloro-N-(5-chloro-2-hydroxyphenyl)acetamide;35588-38-6;MFCD00297054;Acetamide, 2-chloro-N-(5-chloro-2-hydroxyphenyl)-;2-chloro-N-(5-chloro-2-hydroxyphenyl)-acetamide;SCHEMBL247350;VTOWGURRHAVIBF-UHFFFAOYSA-N;DTXSID301248640;BBL028493;STL376643;AKOS002257002;VS-08797;CS-0314856;2-Chloro-N-(5-chloro-2-hydroxyphenyl)acetamide, AldrichCPR

Chemical Property of 2-chloro-N-(5-chloro-2-hydroxyphenyl)acetamide

Chemical Property:

• XLogP3: 2.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 218.9853839
• Heavy Atom Count: 13
• Complexity: 189

Purity/Quality:

98%min ^*data from raw suppliers

2-Chloro-N-(5-chloro-2-hydroxyphenyl)acetamide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1Cl)NC(=O)CCl)O

Technology Process of 2-chloro-N-(5-chloro-2-hydroxyphenyl)acetamide

There total 2 articles about 2-chloro-N-(5-chloro-2-hydroxyphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

chloroacetyl chloride (79-04-9) + 2-hydroxy-5-chloro-aniline (95-85-2) → 2-chloro-N-(5-chloro-2-hydroxyphenyl)acetamide (35588-38-6)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 3h;

DOI:10.1016/j.tetlet.2008.03.120

Reference yield:

→ 2-chloro-N-(5-chloro-2-hydroxyphenyl)acetamide (35588-38-6)

Guidance literature:

Chloressigsaeure, 1.) Keten, 2.) 4-Chlor-2-amino-phenol;

Reference yield: 98.0%

2-chloro-N-(5-chloro-2-hydroxyphenyl)acetamide (35588-38-6) → 5-chloro-2-(chloromethyl)-1,3-benzoxazole (63842-22-8)

Guidance literature:

With toluene-4-sulfonic acid; In phenol; for 3h; Reflux;

upstream raw materials:

chloroacetyl chloride

2-hydroxy-5-chloro-aniline

Downstream raw materials:

6-chloro-2H-1,4-benzoxazin-3(4H)-one

2-chloro-N-(5-chloro-2-hydroxy-3-nitro-phenyl)-acetamide

6-chloro-8-nitro-2H-benzo[b][1,4]oxazin-3(4H)-one

8-amino-2H-benzo[b][1,4]oxazin-3(4H)-one

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