(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1-methyl-2-thioxo-4-imidazolidinone

Base Information

Chemical Name:(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1-methyl-2-thioxo-4-imidazolidinone
CAS No.:154052-53-6
Molecular Formula:C₁₉H₂₆N₂O₂S
Molecular Weight:346.494
Hs Code.:

Synonyms:(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1-methyl-2-thioxo-4-imidazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1-methyl-2-thioxo-4-imidazolidinone

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Technology Process of (Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1-methyl-2-thioxo-4-imidazolidinone

There total 1 articles about (Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1-methyl-2-thioxo-4-imidazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 29181-65-5
1-methyl-2-thioxoimidazolidin-4-one

: 1620-98-0
3,5-di-t-butyl-4-hydroxybenzaldehyde

: 154052-53-6
(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1-methyl-2-thioxo-4-imidazolidinone

Guidance literature:: With acetic acid; 3-amino propanoic acid; for 24h; Heating;
DOI:10.1021/jm00028a017

Reference yield: 70.0%

: 154052-53-6
(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1-methyl-2-thioxo-4-imidazolidinone

: 74-88-4
methyl iodide

: 139226-58-7
(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1,5-dihydro-1-methyl-2-(methylthio)-4H-imidazol-4-one

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In ethanol; for 18h; Ambient temperature;
DOI:10.1021/jm00028a017

Reference yield:

: 154052-53-6
(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-1-methyl-2-thioxo-4-imidazolidinone

: (Z)-<5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-4,5-dihydro-1-methyl-4-oxo-1H-imidazol-2-yl>cyanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / N,N-diisopropylethylamine / ethanol / 18 h / Ambient temperature

2: 51 percent / t-BuOK / ethanol / 2.5 h / Heating

With potassium tert-butylate; N-ethyl-N,N-diisopropylamine; In ethanol;
DOI:10.1021/jm00028a017