Technology Process of C17H16N2O
There total 3 articles about C17H16N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; O,O'-[(R)-(1,1'-binaphthyl-2,2'-diphenolyl)]-N-[(R)-2-methyl-1,2,3,4-tetrahydroquinolinyl]phosphoramidite;
In
tetrahydrofuran;
at 20 ℃;
for 1.5h;
enantioselective reaction;
Schlenk technique;
Inert atmosphere;
DOI:10.1002/anie.201404286
- Guidance literature:
-
With
propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; O,O'-[(R)-(1,1'-binaphthyl-2,2'-diphenolyl)]-N-[(R)-2-methyl-1,2,3,4-tetrahydroquinolinyl]phosphoramidite;
In
tetrahydrofuran;
at 25 ℃;
for 1.5h;
enantioselective reaction;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/jacs.5b10440
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; propylamine; O,O'-[(R)-(1,1'-binaphthyl-2,2'-diphenolyl)]-N-[(R)-2-methyl-1,2,3,4-tetrahydroquinolinyl]phosphoramidite / tetrahydrofuran / 1.5 h / 20 °C / Schlenk technique; Inert atmosphere
With
propylamine; bis(1,5-cyclooctadiene)diiridium(I) dichloride; O,O'-[(R)-(1,1'-binaphthyl-2,2'-diphenolyl)]-N-[(R)-2-methyl-1,2,3,4-tetrahydroquinolinyl]phosphoramidite; sodium hydride;
In
tetrahydrofuran; mineral oil;
DOI:10.1002/anie.201404286
