C₆₁H₄₂

Base Information

Chemical Name:C₆₁H₄₂
CAS No.:1158844-32-6
Molecular Formula:C₆₁H₄₂
Molecular Weight:775.004
Hs Code.:

Synonyms:C₆₁H₄₂

Suppliers and Price of C₆₁H₄₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₁H₄₂

Chemical Property:

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Technology Process of C₆₁H₄₂

There total 7 articles about C₆₁H₄₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1158844-51-9
C₃₃H₄₀B₂O₄

: 23674-20-6
9-bromo-10-phenylanthracene

: 1158844-32-6
C₆₁H₄₂

Guidance literature:: With Aliquat 336; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; toluene; at 100 ℃; for 4h;

Reference yield:

: 98-80-6
phenylboronic acid

: 1158844-32-6
C₆₁H₄₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / toluene; ethanol; water / 12 h / Reflux

2: N-Bromosuccinimide / dichloromethane / 5 h / 20 °C

3: potassium carbonate; Aliquat 336 / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 4 h / 100 °C

With N-Bromosuccinimide; Aliquat 336; sodium carbonate; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; water; toluene;

Reference yield:

: 28320-31-2
2-bromo-9,9-dimethyl-9H-fluorene

: 1158844-32-6
C₆₁H₄₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / toluene; ethanol; water / 12 h / 100 °C

2.1: bromine / dichloromethane / -5 - 25 °C

3.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C

3.2: -78 - 25 °C

4.1: potassium carbonate; Aliquat 336 / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 4 h / 100 °C

With n-butyllithium; bromine; Aliquat 336; sodium carbonate; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene;