2-Hydroxymethyl-4,5-dimethoxy-phenylaethylalkohol

Base Information

Chemical Name:2-Hydroxymethyl-4,5-dimethoxy-phenylaethylalkohol
CAS No.:67645-12-9
Molecular Formula:C₁₁H₁₆O₄
Molecular Weight:212.246
Hs Code.:

Synonyms:2-Hydroxymethyl-4,5-dimethoxy-phenylaethylalkohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Hydroxymethyl-4,5-dimethoxy-phenylaethylalkohol

Chemical Property:

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Technology Process of 2-Hydroxymethyl-4,5-dimethoxy-phenylaethylalkohol

There total 6 articles about 2-Hydroxymethyl-4,5-dimethoxy-phenylaethylalkohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16135-41-4
6,7-dimethoxy-3,4-dihydro-1H-2-benzopyran-3-one

: 67645-12-9
2-Hydroxymethyl-4,5-dimethoxy-phenylaethylalkohol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1.66667h;
DOI:10.1021/acs.orglett.1c04174

Reference yield:

: 6286-46-0
2-bromo-4,5-dimethoxybenzoic acid

: 67645-12-9
2-Hydroxymethyl-4,5-dimethoxy-phenylaethylalkohol

Guidance literature:: Multi-step reaction with 3 steps

2: H₂SO₄ / Heating

3: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; sulfuric acid; In diethyl ether;
DOI:10.1016/S0040-4020(01)96892-9

Reference yield:

: 3809-00-5
4,5-dimethoxyhomophthalic acid

: 67645-12-9
2-Hydroxymethyl-4,5-dimethoxy-phenylaethylalkohol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄ / Heating

2: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; sulfuric acid; In diethyl ether;
DOI:10.1016/S0040-4020(01)96892-9