(2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol

Base Information

Chemical Name:(2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol
CAS No.:1184871-25-7
Molecular Formula:C₄₂H₆₈O₅Si₂
Molecular Weight:709.17
Hs Code.:

(2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol

Synonyms:(2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol

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Chemical Property of (2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol

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Technology Process of (2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol

There total 23 articles about (2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: (2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-2,4-dimethylhex-5-ene-1,3-diol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1184871-25-7
(2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 12h;
DOI:10.1055/s-0037-1610108

Reference yield:

: (2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-[(3S,4S,5R)-6-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,5-dimethylhex-1-enyl]-2,5'-dimethyloctahydro-2,2'-bifuran

: 1184871-35-9
(2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-[(3S,4S,5R,Z)-6-(tert-butyldiphenylsilyloxy)-4-hydroxy-3,5-dimethylhex-1-enyl]-2,5'-dimethyloctahydro-2,2'-bifuran

: 1184871-25-7
(2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; at 20 ℃; for 1.33333h;
DOI:10.1002/anie.200901608

Reference yield:

: 5-{[(2S,2'R,5S,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-2,5'-dimethyloctahydro-2,2'-bifuran-5-yl]methylsulfonyl}-1-phenyl-1H-tetrazole

: 235785-57-6
(2R,3R,4R)-5-(tert-butyldiphenylsilyloxy)-3-(4-methoxybenzyloxy)-2,4-dimethylpentanal

: 1184871-25-7
(2R,3S,4S)-6-((2S,2'R,5S,5'S)-5'-((R)-1-((tert-butyldimethylsilyl)oxy)ethyl)-2,5'-dimethyloctahydro-[2,2'-bifuran]-5-yl)-1-((tert-butyldiphenylsilyl)oxy)-2,4-dimethylhex-5-en-3-ol

: 1184871-34-8
(2S,2'R,5'S)-5'-[(R)-1-(tert-butyldimethylsilyloxy)ethyl]-5-[(3S,4S,5R,Z)-6-(tert-butyldiphenylsilyloxy)-4-(4-methoxybenzyloxy)-3,5-dimethylhex-1-enyl]-2,5'-dimethyloctahydro-2,2'-bifuran

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; toluene; at -78 - 0 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1002/anie.200901608