2,6-[bis-2,5-dimethoxy-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)anilino-N-carbonyl]pyridine

Base Information

• Chemical Name: 2,6-[bis-2,5-dimethoxy-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)anilino-N-carbonyl]pyridine
• CAS No.: 1004783-00-9
• Molecular Formula: C₅₁H₅₉N₃O₂₄
• Molecular Weight: 1098.04

Synonyms:2,6-[bis-2,5-dimethoxy-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)anilino-N-carbonyl]pyridine

Chemical Property of 2,6-[bis-2,5-dimethoxy-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)anilino-N-carbonyl]pyridine

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of 2,6-[bis-2,5-dimethoxy-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)anilino-N-carbonyl]pyridine

There total 1 articles about 2,6-[bis-2,5-dimethoxy-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)anilino-N-carbonyl]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2,6-Pyridinedicarbonyl dichloride (3739-94-4) + 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2,5-dimethoxyaniline (1004782-80-2) + ethanol (64-17-5) → N-carbonyl-(6-ethoxycarbonyl-2-pyridyl)-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2,5-dimethoxyaniline (1004782-99-3) + 2,6-[bis-2,5-dimethoxy-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)anilino-N-carbonyl]pyridine (1004783-00-9)

Guidance literature:

2,6-Pyridinedicarbonyl dichloride; 4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2,5-dimethoxyaniline; With pyridine; In dichloromethane; at 20 ℃; for 2h;

ethanol; In dichloromethane; Further stages.;

DOI:10.1055/S-2007-990856

Reference yield: 80.0%

2,6-[bis-2,5-dimethoxy-4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)anilino-N-carbonyl]pyridine (1004783-00-9) → 2,6-bis[2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone-5-amino-N-carbonyl]pyridine (1004783-16-7)

Guidance literature:

With ammonium cerium(IV) nitrate; In water; acetonitrile; at 20 ℃; for 2h;

DOI:10.1055/S-2007-990856

upstream raw materials:

2,6-Pyridinedicarbonyl dichloride

4-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2,5-dimethoxyaniline

ethanol

Downstream raw materials:

2,6-bis[2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-1,4-benzoquinone-5-amino-N-carbonyl]pyridine

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