{2-[(4-methoxyphenoxy)methyl]-4-(methylethylidene)-5-oxo-2-2,3-dihydrofuryl}methyl decanoate

Base Information

Chemical Name:{2-[(4-methoxyphenoxy)methyl]-4-(methylethylidene)-5-oxo-2-2,3-dihydrofuryl}methyl decanoate
CAS No.:932711-40-5
Molecular Formula:C₂₆H₃₈O₆
Molecular Weight:446.584
Hs Code.:

Synonyms:{2-[(4-methoxyphenoxy)methyl]-4-(methylethylidene)-5-oxo-2-2,3-dihydrofuryl}methyl decanoate

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Chemical Property of {2-[(4-methoxyphenoxy)methyl]-4-(methylethylidene)-5-oxo-2-2,3-dihydrofuryl}methyl decanoate

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Technology Process of {2-[(4-methoxyphenoxy)methyl]-4-(methylethylidene)-5-oxo-2-2,3-dihydrofuryl}methyl decanoate

There total 4 articles about {2-[(4-methoxyphenoxy)methyl]-4-(methylethylidene)-5-oxo-2-2,3-dihydrofuryl}methyl decanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 932711-32-5
5-(hydroxymethyl)-5-[(4-methoxyphenoxy)methyl]-3-(methylethylidene)-4,5-dihydrofuran-2-one

: 2082-76-0
capric anhydride

: 932711-40-5
{2-[(4-methoxyphenoxy)methyl]-4-(methylethylidene)-5-oxo-2-2,3-dihydrofuryl}methyl decanoate

Guidance literature:: With dmap; In dichloromethane; for 0.5h;
DOI:10.1021/jm061289j

Reference yield:

: 932711-31-4
5-[(4-methoxyphenoxy)methyl]-3-(methylethylidene)-5-[(phenylmethoxy)methyl]-4,5-dihydrofuran-2-one

: 932711-40-5
{2-[(4-methoxyphenoxy)methyl]-4-(methylethylidene)-5-oxo-2-2,3-dihydrofuryl}methyl decanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / BCl₃ / CH₂Cl₂ / 2 h / -78 °C

2: 97 percent / dimethylaminopyridine / CH₂Cl₂ / 0.5 h

With dmap; boron trichloride; In dichloromethane;
DOI:10.1021/jm061289j

Reference yield:

: 5-benzyloxymethyl-3-(1-hydroxy-1-methyl-ethyl)-5-(4-methoxy-phenoxymethyl)-dihydro-furan-2-one

: 932711-40-5
{2-[(4-methoxyphenoxy)methyl]-4-(methylethylidene)-5-oxo-2-2,3-dihydrofuryl}methyl decanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.2 g / dimethylaminopyridine / CH₂Cl₂ / 20 °C

2: 88 percent / BCl₃ / CH₂Cl₂ / 2 h / -78 °C

3: 97 percent / dimethylaminopyridine / CH₂Cl₂ / 0.5 h

With dmap; boron trichloride; In dichloromethane;
DOI:10.1021/jm061289j