Technology Process of C17H15FO5S
There total 4 articles about C17H15FO5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium diisopropyl amide;
In
tetrahydrofuran;
at 0 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: acetic acid; pyridinium hydrobromide perbromide; hydrogen bromide / 24 h / 20 °C
2: sulfuric acid / 24 h / Reflux
3: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / Reflux; Inert atmosphere
4: lithium diisopropyl amide / tetrahydrofuran / 1 h / -50 - -40 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); pyridinium hydrobromide perbromide; sulfuric acid; hydrogen bromide; sodium carbonate; acetic acid; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; water; toluene;
DOI:10.1016/j.bioorg.2022.105704
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid / 24 h / Reflux
2: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / Reflux; Inert atmosphere
3: lithium diisopropyl amide / tetrahydrofuran / 1 h / -50 - -40 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); sulfuric acid; sodium carbonate; lithium diisopropyl amide;
In
tetrahydrofuran; ethanol; water; toluene;
DOI:10.1016/j.bioorg.2022.105704
