10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one

Base Information

Chemical Name:10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one
CAS No.:228405-26-3
Molecular Formula:C₃₂H₄₆O₃Si₂
Molecular Weight:534.886
Hs Code.:

10-(<i>tert</i>-butyl-dimethyl-silanyloxy)-1-(<i>tert</i>-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one

Synonyms:10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one

Suppliers and Price of 10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one

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Technology Process of 10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one

There total 6 articles about 10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 75859-97-1
4-t-butyldimethylsilyloxy-2-butynal

: 228405-25-2
[6-(t-butyldiphenyl-silyl)oxy]-2-oxohexylphosphonic acid dimethyl ester

: 228405-26-3
10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran;
DOI:10.1016/S0040-4039(99)00579-1

Reference yield:

: 542-28-9,26354-94-9
3,4,5,6-tetrahydro-2H-pyran-2-one

: 228405-26-3
10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one

Guidance literature:: Multi-step reaction with 4 steps

1: 83 percent / Et₃N

2: 95 percent / imidazole / dimethylformamide

3: 94 percent / n-BuLi / tetrahydrofuran

4: 79 percent / t-BuOK / tetrahydrofuran

With 1H-imidazole; n-butyllithium; potassium tert-butylate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(99)00579-1

Reference yield:

: 14273-92-8
methyl 5-hydroxypentanoate

: 228405-26-3
10-(tert-butyl-dimethyl-silanyloxy)-1-(tert-butyl-diphenyl-silanyloxy)-dec-6-en-8-yn-5-one

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / imidazole / dimethylformamide

2: 94 percent / n-BuLi / tetrahydrofuran

3: 79 percent / t-BuOK / tetrahydrofuran

With 1H-imidazole; n-butyllithium; potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(99)00579-1