Technology Process of C24H24N2O4
There total 5 articles about C24H24N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C36H29N3O4;
With
pyridinium p-toluenesulfonate;
In
methanol;
at 20 ℃;
for 10h;
With
hydrogenchloride;
In
methanol; water;
at 20 ℃;
for 0.5h;
DOI:10.1002/anie.201201905
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoroacetic acid / 0.5 h / 20 °C
2.1: triethylsilane / 2 h / 0 - 20 °C
3.1: (R)-3,3'-bis(3,5-dinitrophenyl)-1,1'-binaphthyl-2,2'-dicarboxylic acid / 1,3,5-trimethyl-benzene / 24 h / -20 °C / Molecular sieve
4.1: pyridinium p-toluenesulfonate / methanol / 10 h / 20 °C
4.2: 0.5 h / 20 °C
With
triethylsilane; (R)-3,3'-bis(3,5-dinitrophenyl)-1,1'-binaphthyl-2,2'-dicarboxylic acid; pyridinium p-toluenesulfonate; trifluoroacetic acid;
In
methanol; 1,3,5-trimethyl-benzene;
3.1: Ugi-type reaction;
DOI:10.1002/anie.201201905
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoroacetic acid / 0.5 h / 20 °C
2.1: triethylsilane / 2 h / 0 - 20 °C
3.1: (R)-3,3'-bis(3,5-dinitrophenyl)-1,1'-binaphthyl-2,2'-dicarboxylic acid / 1,3,5-trimethyl-benzene / 24 h / -20 °C / Molecular sieve
4.1: pyridinium p-toluenesulfonate / methanol / 10 h / 20 °C
4.2: 0.5 h / 20 °C
With
triethylsilane; (R)-3,3'-bis(3,5-dinitrophenyl)-1,1'-binaphthyl-2,2'-dicarboxylic acid; pyridinium p-toluenesulfonate; trifluoroacetic acid;
In
methanol; 1,3,5-trimethyl-benzene;
3.1: Ugi-type reaction;
DOI:10.1002/anie.201201905
