4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate

Base Information

Chemical Name:4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate
CAS No.:405157-55-3
Molecular Formula:C₃₈H₄₉NO₈
Molecular Weight:647.809
Hs Code.:

Synonyms:4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate

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Chemical Property of 4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate

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Technology Process of 4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate

There total 11 articles about 4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 405157-53-1
4''-[10-(tert-butyloxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate

: 405157-55-3
4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 13h;
DOI:10.1021/ma010290j

Reference yield:

: 2834-05-1
11-bromoundecanoic acid

: 405157-55-3
4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / conc. H₂SO₄ / CH₂Cl₂ / 15 h / 20 °C

2: 92 percent / K₂CO₃ / 18-crown-6 / acetone / 36 h / 60 °C

3: 98 percent / H₂ / 10 percent Pd/C / ethyl acetate / 20 °C

4: 72 percent / N,N'-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / 20 °C

5: 95 percent / trifluoroacetic acid / CH₂Cl₂ / 13 h

With dmap; sulfuric acid; hydrogen; potassium carbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; 18-crown-6 ether; In dichloromethane; ethyl acetate; acetone;
DOI:10.1021/ma010290j

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 405157-55-3
4''-[10-(hydroxycarbonyl)decyloxy]phenyl 4-[4'-(2-(R)-octyloxy)-3'-nitrophenyl]benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / K₂CO₃ / 18-crown-6 / acetone / 36 h / 60 °C

2: 98 percent / H₂ / 10 percent Pd/C / ethyl acetate / 20 °C

3: 72 percent / N,N'-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / 20 °C

4: 95 percent / trifluoroacetic acid / CH₂Cl₂ / 13 h

With dmap; hydrogen; potassium carbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; palladium on activated charcoal; 18-crown-6 ether; In dichloromethane; ethyl acetate; acetone;
DOI:10.1021/ma010290j