benzoic acid trifluoromethyl ester

Base Information

Chemical Name:benzoic acid trifluoromethyl ester
CAS No.:1035797-66-0
Molecular Formula:C₈H₅F₃O₂
Molecular Weight:190.122
Hs Code.:

Synonyms:benzoic acid trifluoromethyl ester

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Chemical Property of benzoic acid trifluoromethyl ester

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Technology Process of benzoic acid trifluoromethyl ester

There total 6 articles about benzoic acid trifluoromethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 353-50-4
Carbonyl fluoride

: 618-32-6
Benzoyl bromide

: 4124-31-6
trichloroacetic acid anhydride

: 1035797-66-0
benzoic acid trifluoromethyl ester

Guidance literature:: trichloroacetic acid anhydride; With potassium fluoride; 18-crown-6 ether; In tetrahydrofuran; acetonitrile; at -78 - 80 ℃; Sealed tube; Glovebox; Inert atmosphere;

Carbonyl fluoride; In tetrahydrofuran; acetonitrile; at -78 ℃; for 2h; Sealed tube; Glovebox;

Benzoyl bromide; In tetrahydrofuran; acetonitrile; at 30 ℃; for 2h; Reagent/catalyst; Sealed tube; Glovebox; Inert atmosphere;

Reference yield: 42.0%

: 618-32-6
Benzoyl bromide

: 3582-05-6
trifluoromethyl trifluoromethanesulfonate

: 455-32-3
benzoyl fluoride

: 1035797-66-0
benzoic acid trifluoromethyl ester

Guidance literature:: trifluoromethyl trifluoromethanesulfonate; With silver fluoride; In acetonitrile; at -30 ℃; for 2h; Inert atmosphere;

Benzoyl bromide; In acetonitrile; at -30 - 20 ℃; for 24.5h; Inert atmosphere; Darkness;
DOI:10.1016/j.jfluchem.2009.11.006